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High-Temperature Vacuum Furnaces VHT with Graphite, Molybdenum or MoSi2 Heating
 
VHT 8/22-GR VHT 40/22-GR  

Graphite heating chamber

Molybdenum heating chamber

Chamber made of ceramic fiber

VHT gas supply diagram, automatic operation

N2-emergency purge system and torch for H2-operation

Single-stage rotary vane pump for heat treatment in a rough vacuum to 20 mbar

Turbo-molecular pump with booster pump for heat treatment in a vacuum to 10-5 mbar

VHT gas supply diagram, debinding and sintering

The compact furnaces of the VHT line are available as electrically heated chamber furnaces with graphite, molybdenum or MoSi2 heating. A wide variety of heating designs as well as a complete range of accessories allow optimal furnace configuration for technically demanding customer processes. The vacuum-tight retort enables heat treatment processes either in protective and reaction gas atmospheres or in a vacuum, depending on the application, all the way to 10-5 mbar. With the appropriate safety technology, the furnaces are also suitable for operation with hydrogen.

Heating Concepts

Graphite – VHT ../GR

  • Suitable for processes under protective and reaction gases or under vacuum
  • Tmax 1800 °C and 2200 °C
  • Graphite felt insulation
  • Temperature measurement using type B thermocouple (version to 1800 °C)
  • Temperature measurement using optical pyrometer (version to 2200 °C)

Molybdenum – VHT ../MO

  • Suitable for processes under highly pure protective and reaction gases or under a high vacuum up as much as 10-5 mbar
  • Tmax 1600 °C
  • Insulation made of Molybdenum steel sheets

MoSi2 – VHT ../KE

  • Suitable for processes under protective and reaction gases or in air or under vacuum
  • Tmax 1800 °C
  • Insulation made of high purity aluminum oxide fiber

Basic Version VHT (All Heating Concepts)

  • Standard furnace sizes 8, 40 and 100 liters
  • A water-cooled stainless steel process reactor sealed with temperature-resistant o-rings
  • Frame made of stable steel profiles, easy to service due to easily removable stainless steel panels
  • Casing of the VHT 8 model on castors for easy repositioning of furnace
  • Cooling water manifold with manual stopcocks in supply and return lines, automatic flowmeter monitoring, open-loop cooling water system
  • Adjustable cooling water circuits with flowmeter and temperature indicator and overtemperature fuses
  • Switchgear and controller integrated in furnace housing
  • H 700 PLC control with clearly laid out 5.7" touchpanel control for program entry and display, 10 programs each with 20 segments
  • Over-temperature limit controller with manual reset for thermal protection class 2 in accordance with EN 60519-2
  • Manual operation of the process gas and vacuum functions
  • Manual gas supply for one process gas (N2 or Ar) with adjustable flow
  • Bypass with manual valve for rapid filling or flooding of furnace chamber
  • Manual gas outlet with overflow valve (20 mbar relative)
  • Single-stage rotary vane pump with ball valve for pre-evacuating and heat treatment in a rough vacuum to 5 mbar
  • Pressure gauge for visual pressure monitoring

Additional equipment

  • Housing, optionally separable, for passing through narrow door openings
  • Manual gas supply for second process gas (N2 or Ar) with adjustable flow and bypass
  • Molybdenum or carbon-fiber-carbon retort with direct gas supply for clean atmosphere and improved temperature uniformity in the furnace chamber
  • Charge thermocouple with display
  • Two-stage rotary vane pump with ball valve for pre-evacuating and heat-treating in a vacuum to 10-2 mbar
  • Cooling unit with closed-loop cooling water circuit

The use of automatic valves for process gas or exhaust air management and the powerful H 3700 controller allow the entire heat treatment process to be run fully automatically. The entry of all process data (temperatures, ramps, gas supply and vacuum) is easily controllable from a large, 12" graphic control panel. System status with all process-related data are clearly shown on a process control diagram. All valves and the vacuum pump can also be operated manually from here as well. The system has an automatic pre-program and post-program for purging the furnace chamber and also features automated leak testing.

Automatic Version VHT
  • Features the same as basic version of VHT, plus:
  • Automatic gas supply for one process gas (N2 or Ar) with adjustable flow
  • Bypass for rapid filling or flooding of furnace chamber
  • Automatic gas outlet with check valve and pressure relief valve (20 mbar)
  • Single-stage rotary vane pump with check valve for pre-evacuating and heat treatment in a rough vacuum to 20 mbar
  • Transducer for absolute and relative pressure measurements
  • H3700 controller (10 programs with 20 segments each)
  • Operation with 12" graphical control panel (touchpanel)

Additional equipment

  • Mass flow controller for varying flow volumes and generating gas mixtures (with second process gas)
  • Furnace pressure control with position-controlled exhaust valve (partial pressure control)
  • Electric or gas-heated exhaust gas torch for process gas post-combustion
  • Water-cooled exhaust gas cooler
  • Condensate traps for separation of large amounts of binder
  • Two-stage rotary vane pump with check valve for pre-evacuating and heat treatment in a vacuum to 10-2 mbar
  • Pump stand with turbo-molecular pump and slide valve for pre-evacuating and for heat treatment in a vacuum to 10-5 mbar (only for molybdenum model) including electric pressure transducer and booster pump
  • PC control via NCC with enhanced optional documentation and possible connection to customer LAN
Extension Package – Hydrogen in VHT-MO and VHT-GR

When hydrogen is used as a process gas, our systems come equipped with additional safety technology. Only certified and industry proven safety sensors are used. The furnaces are always controlled using a fail-safe controller (S7-300F/safety controller). The controller and documentation are carried out using Nabertherm Control Center NCC (see page 42).

Two Temperature-Dependent Concepts Available for Safe Operation with Hydrogen:

  • Partial pressure operation: H2 infeed under controlled negative pressure (partial pressure) in the process reactor starting from 750 °C furnace chamber temperature
  • Atmospheric operation: H2-purging of process reactor starting from room temperature at controlled over pressure (50 mbar relative)

Automatic Version VHT for Operation with Hydrogen

  • Features as found with automatic version of the VHT without hydrogen operation, plus
  • Redundant process gas valves for hydrogen
  • Monitored pre-pressures of all process gases
  • Bypass for safe purging of furnace chamber with inert gas
  • Pressure-monitored emergency flooding with automated solenoid valve opening
  • Electric or gas-heated exhaust gas torch for H2 post-combustion
 VHT ...-18/GRVHT ...-16/MOVHT ...-18/KE
Inert gas
Airto 400 °C-
Hydrogen-
Rough vacuum and fine vacuum (>10-3 mbar)
High vacuum (<10-5 mbar)--
ModelTmaxInner dimensions in mmVolumeOuter dimensions in mmSupplyElectricalWeightMaterial heater/
 °CWDHin lWDHpower/kWconnection*in kginsulation
VHT 8/18-GR180017024020081250 (800)¹1100200027,0three-phase1200Graphite/graphite felt
VHT 40/18-GR18003004503004015002000230083,0three-phase2000Graphite/graphite felt
VHT 100/18-GR1800450550450100175022002600on requestthree-phase2800Graphite/graphite felt
             
VHT 8/22-GR220017024020081250 (800)¹1100200027,0three-phase1200Graphite/graphite felt
VHT 40/22-GR22003004503004015002000230083,0three-phase2000Graphite/graphite felt
VHT 100/22-GR2200450550450100175022002600on requestthree-phase2800Graphite/graphite felt
             
VHT 8/16-MO160017024020081250 (800)¹1100200034,0three-phase1200Molybdenum
VHT 40/16-MO160030045030040150020002300122,0three-phase2000Molybdenum
VHT 100/16-MO1600450550450100175022002600on requestthree-phase2800Molybdenum
             
VHT 8/18-KE180017024020081250 (800)¹1100200012,5three-phase1200MoSi2/ceramic fiber
VHT 40/18-KE18003004503004015002000230045,0three-phase2000MoSi2/ceramic fiber
VHT 100/18-KE1800450550450100175022002600on requestthree-phase2800MoSi2/ceramic fiber
¹With the switching system unit removed *See page 42 for information about supply voltage.

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